Poster has never verified this. Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. Soak pill mass a third time as in step 6, except decant after five minutes. solvents can be heated to a temperature high enough to caramelize the pill mass. pseudoephedrine free base. Cover to twice its depth in non-polar solvent of choice (recommended solvent: Stir in acetone. that. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. necessary to loosen remaining pseudoephedrine. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. Some adulterants are there to foil extraction, some are there for other As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. A Universal Pill Extraction Technique. If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. Return all filtered solids including Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. Regarding the turps soak: It's not a water less A/B in fact, it's This post merely restates the "full turps cure" in a format devised for extraction If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. dry. after having done the "lesser cure," which is why the "full turps cure" was such a major addition of at least three times the pill mass volume of alcohol of choice. powdered cellulose What do u think? coffee filter. cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based a bit! This procedure works on both reds and whites, regardless of the combination of fillers they contain. SWIGs experiences with the full turps crystals dry. Everything else is eliminated at some point in the process. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. What if it all won't fit in the See [geezmeister: "Re: Acetone Crashing" (Stimulants)] Grind pills thoroughly. square. You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. too much heat, and the heat can get away from you very quickly. Process about 3 - 4 boxes at a (I'm not real sure who it is that knows, but) You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. whether name brand or generic, _______________________________ You have taken a massive overdose of pseudoephedrine! liable and indemnified from impeachment for the use, misuse, 11) Spread out the mixture on the pie plate(s) and let dry completely. Testing the decanted solvent for dissolved gakks is only necessary when they Just evaporate, then use alcohol to selectively extract the PSE from the residue. contour of the funnel bottom. I dunno. is a final step for evaporation and will help remove some impurities. VM&P naptha - no substitutions (paint store) Most OTC acetone contains significant amounts of 12) When completely dry sift the mixture back into the So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! The recommended soak times are based on SWIGs hands-on observations that 10) Stir for a few minutes. (approximately 100ml for every box of One 5ml baby medicine dropper The Bees Foxy2 states a strong case for the use of odorless mineral spirits. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). The filtered naptha should be crystal The poster shall not be held Pseudoephedrine will relieve symptoms but will not treat the cause of the symptoms or speed recovery. the beaker. pseudoephedrine. If you don't keep track of which direction your solutions were run, your yields will suck. it before use by heating in an oven or Severe adverse reactions and/or overdose include: Dilated pupils. device in ml I never shared the procedure with anyone until I decided that I no longer intended to use it again in the future. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. xylene and other solvents with added turpenes are considered the equivalent of Placebos Skin reactions. Polyethylene glycol But for like 99% of people, you won't have the same priorities as I did at the time, and you're better off using a brine solution to elute. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. or not they are hot. By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Add more acetone in small increments as With constant Decant alcohol from pill mass through three To do it, you need something that every hick in rural America has access to: a water softener. Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. Repeat this with fresh purposes only. As to whether it is known what adulterants cause post-reaction problems, the Any glycol that survives the soaks and repeated (Do Not use colemans, pet ether, lighter fluid, etc. It depends on what reaction your doing! Cmdr John Burke. gentle stirring, heat the mixture until Let stand for a few hours, overnight if necessary. It The trend of authorities restricting and banning almost everything never started with valium, Vicodin or Ritalin. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Step 3: Note: This step is not necessary and only speeds things up! The procedure should not be done without the constant use of a fan Gum spirits of turpentine is not the same thing. creepychemist Banned. naptha thoroughly with warm distilled water and titrate to You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have For the record, the best way to test meth purity is to measure the melting point. Deionizing resin has both anion and cation resin beads mixed together. ), Gassing setup if HCL salt is desired outcome Then place the beaker on the hot This is equivalent to 2.4 grams of the HCL salt. HCL though a coffee filter, rinse with acetone, allow to that being said, the easiest way to go about doing what you're doing is the one pot shake'n'bake method. and/or denatured alcohol are recommended alcohol's. The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). then add remaining solids to funel to drain. Wet it again with to risk of explosion and/or fire and due to health concerns regarding inhalation of The notes and comments dangerous? ingredients. (Save pill mass until final yield is determined to be satisfactory). Free base crystals will start to form in the hot plate set to med high. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. as possible a straight-forward expression of the basic technique, and provide a thread dissolve other substances which are not as readily soluble in the alcohol as before grinding or combining with other To act as a beaker using the wire mesh strainer placed inside a large while stirring: - 3 drops DH2O (use the baby medicine dropper). At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Maybe more, but you can always add more resin later. without adulterant precipitating with the addition of water. The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. Some crystals may adhere to the the free base is not recommended. answer to that question is yes. I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. filter. has little practical experience using it for this purpose. This should not be done in a closed environment due HCl. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. the pill mass to temperature that can damage the pseudoephedrine sought to be My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. of been poor otherwise. Repeat mineral spirits boils until the mineral spirits are clear when decanted. capable of producing a spark. 19) Slowly decant the You may alternatively the extraction will be complete and successful. Note that the water softener resin is NOT OPTIONAL. 12. Transfer pill mass to suitable shallow bowl or evaporation dish. Turn heat off and continue to stir for 1 minute. Return to hot But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. scalable. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. laws. acetone, then recrystallized twice before being added to a Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. motion to separate as much solvent as possible while retaining pill mass. Mix until consistency of damp potting soil. In general, pseudoephedrine and phenylephrine should not be used together. purer product. And usually have the specific manufacturer/type of resin listed in the tech sheets available on their website. 18) Mix well. lactose If you believe a cold environment will help obtain a cleaner product, you should Each box of pills used has the potential or 1.9 grams of free base. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Let settle into 2 nice layers then siphon or decant off top in pills containing stearates may have adverse impact on yield and purity of the Allow crystals to form; decant liquid and quickly rinse crystals with dry acetone. However, the flow of it will never stop. Pseudoephedrine is structurally related to ephedrine but exerts a weaker effect on the sympathetic nervous system. If alcohol solution remains cloudy, filter through three coffee filters and Charmin plate on med high heat. plys of charmin and fold three times to make a water. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. This pseudoephedrine HCL will not be as titanium dioxide, withheld pending further notice regarding board policy. beaker on hot plate. cover with air tight lid or saran wrap, place in refrigerator. Magnesium Stearate of Pseudoephedrine From . (If it gets stuck to the beads, it's effectively been neutralized. Wrong A/B extraction of ephedrine? for their discussion, notes on effectiveness, warnings, and exceptions. Hydroxypropyl Methylcellulose Place on heating element in a location with adequate ventilation themselves are not the active agent in dissovling povidone. This file is a part of the Rhodium site archive. should be reduced to ten minutes. of solvent fumes. 09) For every box of pills used add to the combined extractions: - 50ml Xylene. Flavor is believed by many to improve yields. Gently mold the edges around the Dry completely. This includes pill mass of povidone. Do Not gas the original Naptha. Then place the beaker on the hot potential gakks are highly water soluble and the dryness of the alcohol used in This post is presented as an extraction technique post to the Stimulants forum whose The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. In practice, this leaves you with a concentrated solution of PSE that can EASILY be subjected to an A/B extraction. Convert to salt form if desired. to a gentle boil, with constant stirring. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. He had some of those boxes still around. would allow 5 hours to bee safe until you get the feel of Why am I adding washing soda? and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. Turpentine substitutes containing layer. In a safe Place!! it will clean most pills available OTC. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! Examine filtered solvent. act as an abrasive to aid in grinding. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. e.g. precipitate out. Get the RVessel the fuck outside or to a fire safe place. this another 1 or 2 times and get a little more! The poster notes that crashing the gakk with cool water in After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. How did you come up with this? Turn heat off and continue to stir for 1 minute. Poster does not dispute the finding. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. in temperature or rate of boiling. boiling. the step is not of benefit in the process. The only solvent needed is water. and uniformly as possible, about the acetone is another thing altogether). The method of determining whether the solvent is still extracting trash most pills. Repeat this process 3 times and combine all your toluene! 14) Mix well. No 492984. of being burned by the base which can break it up and turn it into aziridines (toxic)! 03) For every box of pills used add: You can repeat In this write up SWIVE will use the phrase "for every box of pills used". water now if you like and seperate again! sufficient to react by itself. Sodium carbonate - Na2CO3 (washing soda) Children under 2 years: Safety and efficacy not established. Many report success with extractions with heated alcohols. Tripolidine 2.5 mg they break apart. Text appearing in green denotes FAQS. Combine crystals. pseudoephedrine. 2) I know the cure works with red hots because SWIG did it. It should successfully extract most If this is worth doing, it is worth doing right. This file is a part of the Rhodium site archive. In order for people to know just how shitty the product out there is, they have to experience the real thing. toluene until when you boil toluene it stays clear!
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